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PII: S0921-4526(99)00068-X
Copyright © 1999 Published by Elsevier Science B.V. All rights reserved.


    Investigation of magnetic coupling phenomena in
    Fe1-xCrx/Cr-superlattices with spin-polarized neutrons

R. SiebrechtCorresponding Author Contact Information <#m4.cor*>, E-mail
The Corresponding Author <mailto:siebrech@ill.fr>, a <#orfa>, b <#orfb>,
A. Schreyera <#orfa>, c <#orfc>, T. Schmittea <#orfa>, W. Schmidtb
<#orfb> and H. Zabela <#orfa>

a Institut für Festkörperphysik, Ruhr-Universität Bochum, 44780 Bochum,
Germany
b Institut Laue¯Langevin, 38042 Grenoble cedex 9, France
c NIST Center for Neutron Research, Gaithersburg, MD 20899, USA

Available online 10 January 2000.


    Abstract

We present the results of temperature dependent measurements of
magnetically coupled Fe1-xCrx/Cr-superlattices. These results are
supplementary to the ones known for non-collinearly coupled
Fe/Cr-superlattices. By systematically varying the Cr concentration x we
cover a wide range of the Fe1-xCrx-phase diagram. As an experimental
technique spin-polarized neutron reflectivity with spin analysis and
high-angle neutron scattering proves to be ideal for this work.

Author Keywords: Magnetic exchange coupling; Curie temperature; Néel
temperature; Neutron reflectivity


    Article Outline

1. Introduction
2. Samples
3. Experimental
4. Results
5. Conclusions
Acknowledgements
References



Enlarge Image
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(22K)
Fig. 1. Reflectivity measurement with spin-polarized neutrons and spin
analysis at T=35 K for a Fe0.43Cr0.57/Cr sample. The half order Bragg
peak in R+-(=R-+) and no intensity splitting at the chemical first order
Bragg peak position in R++ and R-- indicate an AFM coupling
perpendicular to the neutron polarisation axis. The high intensity in
R++ and R-- at the half order position is related to a high diffuse
magnetic scattering which was confirmed with off specular scans. The
inset documents the magnetic reorientation from AFM to FM by its
temperature-dependent splitting. For more details see text.

Table 1. List of [Cr/Fe1-xCrx]N/Cr/Nb/(1 Not-found 0 2)Al2O3 samples
with systematic variation of the Cr concentration x. The samples were
grown under equivalent conditions by molecular beam epitaxy. The spacer
layer thicknesses, tCr<45 Å, was chosen to assure a commensurate AF spin
structure. The large number of superlattice periods increases the amount
of Cr which improves the signal to background ratio in neutron
scattering experiments. The measured Curie temperatures for samples with
higher concentrations are considerably lower than the bulk values View
Table
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(<1K)


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