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Physica B: Condensed Matter
Volume 335, Issues 1-4 , July 2003, Pages 77-81

Proceedings of the Fourth International Workshop on Polarised Neutrons for Condensed Matter Investigations

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doi:10.1016/S0921-4526(03)00195-9    How to Cite or Link Using DOI (Opens New Window)  
Copyright © 2003 Elsevier Science B.V. All rights reserved.

Measuring lateral magnetic structures in thin films using time-of-flight polarized neutron reflectometry

W. -T. LeeCorresponding Author Contact Information, E-mail The Corresponding Author, a, 1, F. Klosea, 1, H. Q. Yinb and B. P. Topervergc, d

a Oak Ridge National Laboratory, Oak Ridge, TN 37831, USA
b University of Alabama, Tuscaloosa, AL 35487, USA
c Forschungszentrum Jülich, Jülich D-52425, Germany
d Petersburg Nuclear Physics Institute, Gatchina 188300, Russia

Available online 22 May 2003.


Abstract

Polarized neutron reflectometry (PNR) has recently been applied to study lateral magnetic structures such as regular micron-sized magnetic arrays on a surface. To date, however, there is a lack of detailed accounts of the features observed in the scattered intensity map in the special case of time-of-flight (TOF) PNR. We present here preliminary measurement results on lithographically produced arrays of micron-sized rectangular permalloy magnetic bars. The measurements demonstrate the potential of the method to provide detailed structural information on a laterally patterned sample, as well as on its magnetic characteristics. The information can be obtained by analyzing the specular reflection along with three off-specular Bragg sheets. Most of the features seen experimentally can be interpreted by using simple heuristic arguments. In addition, we also present results of a study of lateral magnetic domains in an exchange-biased Co/CoO bilayer film to illustrate the capability of TOF PNR in the study of large lateral magnetic domains in the case when almost no off-specular scattering is detected.

Author Keywords: Time-of-flight neutron reflectometry; Off-specular scattering; Specular reflection; Distorted-wave Born approximation; Patterned magnetic arrays; Lateral magnetic domains

PACS classification codes: 61.12.Ha; 61.10.Bt; 75.70.Kw; 75.70.Cn


Article Outline

• Acknowledgements
• References



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Fig. 1. AFM image of the micron-sized magnetic elements on a silicon surface.

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Fig. 2. Log-scale intensity map for (a) spin-up and (b) spin-down incident neutrons scattered from an array of micron-sized magnetic elements on a silicon surface. The solid line at 1.08° is the horizon. The dotted lines are calculated locations of: (1) specular reflection; (2, 3) off-specular reflections; and (4) diffraction. The dashed lines are the critical edges (from the horizon to higher/lower angles): the silicon edge (above the horizon only) and the permalloy edges corresponding to SLD Nbc+ and Nbc−.

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Fig. 3. Reflectivities of an exchange-biased CoO/Co bilayer at 10 K: (a) R+ (filled symbols) and R (open symbols) at H=+200 Oe (circle), +450 Oe (square), and +5 kOe (lower triangle); (b) R−+ at H=+200 Oe (filled circle), +450 Oe (square), +5 kOe (lower triangle), and R−+(90°) (upper triangle). The inset in (a) shows the hysteresis (solid line) at 10 K and the normalized magnetization obtained from R+ and R. (c) Magnetic domain dispersion small chi, Greek2 of the CoO/Co bilayer at 10 K and H=+200 Oe (filled circle), and +450 Oe (square). Data taken at reversal at +350 Oe is included for comparison (upper triangle).

References

1. J.F. Ankner and G.P. Felcher. J. Magn. Magn. Mater 200 (1999), p. 741. SummaryPlus | Full Text + Links | PDF (739 K)

2. C.F. Majkrzak. Physica B 221 (1996), p. 342. Abstract | PDF (1061 K)

3. H. Zabel, R. Siebrecht and A. Schreyer. Physica B 276 (2000), p. 17. SummaryPlus | Full Text + Links | PDF (226 K)

4. B.P. Toperverg. Physica B 297 (2001), p. 160. SummaryPlus | Full Text + Links | PDF (142 K)

5. B.P. Toperverg, G.P. Felcher, V.V. Metlushko, V. Leiner, R. Siebrecht and O. Nikonov. Physica B 283 (2000), p. 149. SummaryPlus | Full Text + Links | PDF (180 K)

6. B.P. Toperverg, Polarized Neutron Reflection and Off-Specular Scattering in Polarized Neutron Scattering, Forschungszentrum Jülich, Series "Matter and Materials", Vol. 12, 2002.

7. W.-T. Lee, S.G.E. te Velthuis, G.P. Felcher, F. Klose, T. Gredig, D. Dahlberg, Phys. Rev. B 65(22) (2002); art. no. 224417.

8. E.C. Stoner and E.P. Wohlfarth. Philos. Trans. R. Soc. London Ser. A 240 (1948), p. 599.


Corresponding Author Contact InformationCorresponding author. Tel.: +1-630-252-5285; fax: +1-630-252-4163

1 Current address: Argone National Laboratory, IL 60439, USA.



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Physica B: Condensed Matter
Volume 335, Issues 1-4 , July 2003, Pages 77-81
Proceedings of the Fourth International Workshop on Polarised Neutrons for Condensed Matter Investigations


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